High pressures and temperatures cause materials to exhibit unusual properties, some of which can be special. Understanding such new properties is important for developing new materials for desired industrial uses and also for understanding the interior of Earth, where everything is hot and squeezed.
A paper in Nature Geoscience highlights a new technique in which small amounts of a sample can be studied while being hot and squeezed within an electron microscope. Use of such a microscopy method permits determination of details down to the scale of a few atoms, including the detection of unexpected atom types or atoms in unexpected places, as within a mineral.
Jun Wu and Peter Buseck, the paper's authors, both at Arizona State University, conducted the research on campus at the J.M. Cowley Center for High Resolution Electron Microscopy of the LeRoy Eyring Center for Solid State Science. The researchers used tiny containers of carbon, less than one-thousandth the width of a human hair and therefore small enough to fit within high-resolution electron microscopes, to enclose materials similar to those deep within Earth. They then used the electron beam to shrink and thereby squeeze these minuscule capsules. When combined with heating of the samples, new features were observed in the enclosed materials.
"Under such high pressures and temperatures, the materials inside the capsules developed faults that concentrated carbon along them," explains Buseck, Regents' Professor in the Department of Chemistry and Biochemistry and the School of Earth and Space Exploration.
The Nature Geoscience paper describes the use of this new method to address the important problem of how and where carbon is located within Earth's interior. Carbon is an essential building block for all forms of life and it also has important effects on climate and climate change through greenhouses gases such as carbon dioxide and carbon tetrahydride, also known as natural gas or methane.
The largest single reservoir for carbon is within Earth's interior. However, the known hosts for this carbon are believed to be insufficient to explain the amounts present.
Because Earth's interior (as well as the interiors of other planets) contains vast amounts of materials like those used in the experiments, the scientists conclude that such faults, and the carbon they concentrate, provide a solution to the problem of explaining where large amounts of carbon reside in Earth's interior.
Wu and Buseck's experiments also demonstrate a new way of studying materials at high pressure and temperature within an electron microscope, thereby significantly extending the tools available to scientists for examining materials under extreme conditions.
Nicole Cassis | EurekAlert!
Impacts of mass coral die-off on Indian Ocean reefs revealed
21.02.2017 | University of Exeter
How much biomass grows in the savannah?
16.02.2017 | Friedrich-Schiller-Universität Jena
In the field of nanoscience, an international team of physicists with participants from Konstanz has achieved a breakthrough in understanding heat transport
Cells need to repair damaged DNA in our genes to prevent the development of cancer and other diseases. Our cells therefore activate and send “repair-proteins”...
The Fraunhofer IWS Dresden and Technische Universität Dresden inaugurated their jointly operated Center for Additive Manufacturing Dresden (AMCD) with a festive ceremony on February 7, 2017. Scientists from various disciplines perform research on materials, additive manufacturing processes and innovative technologies, which build up components in a layer by layer process. This technology opens up new horizons for component design and combinations of functions. For example during fabrication, electrical conductors and sensors are already able to be additively manufactured into components. They provide information about stress conditions of a product during operation.
The 3D-printing technology, or additive manufacturing as it is often called, has long made the step out of scientific research laboratories into industrial...
Nature does amazing things with limited design materials. Grass, for example, can support its own weight, resist strong wind loads, and recover after being...
Nanometer-scale magnetic perforated grids could create new possibilities for computing. Together with international colleagues, scientists from the Helmholtz Zentrum Dresden-Rossendorf (HZDR) have shown how a cobalt grid can be reliably programmed at room temperature. In addition they discovered that for every hole ("antidot") three magnetic states can be configured. The results have been published in the journal "Scientific Reports".
Physicist Dr. Rantej Bali from the HZDR, together with scientists from Singapore and Australia, designed a special grid structure in a thin layer of cobalt in...
13.02.2017 | Event News
10.02.2017 | Event News
09.02.2017 | Event News
22.02.2017 | Physics and Astronomy
22.02.2017 | Life Sciences
21.02.2017 | Earth Sciences