A doctoral thesis carried out by Jorge Juan Soto Chinchilla, from the Department of Analytical Chemistry at the University of Granada (Universidad de Granada), and directed by professors Ana María García Campaña and Laura Gámiz Gracia, proposes new analysis methods for the detection of pesticide residue (carbamates) and antibiotic residue (sulfonamides) in water, plant foods and food of animal origin (milk and meats from varied sources). These new methods constitute a routine analysis alternative to the analysis used until now. Research forms part of several projects financed by the Spanish National Institute for Agrarian and Alimentary Research (INIA) and the Ministry of Education and Science, in collaboration with the company Puleva Biotech.
The main goal of the work “New analytical methodologies, under quality criteria, for the determination of pharmaceutical residues in waters and food”, carried out by the research group “Quality in Food, Environmental and Clinical Analytical Chemistry (FQM-302)”, has been to develop new methods to detect residues in food of these contaminants below the Maximum Residue Levels (MRL) established by the European Union, in order to guarantee the quality of the product and permit its distribution and consumption. Researchers point out, regarding water, that “the interest caused by control of residue levels of pesticides, which can be found in water as a result of treatment of crops with such compounds, is widely known. ”However, concern on detecting pharmaceutical residue, specifically antibiotic, is quite recent. The presence of these contaminants in fresh waters can cause a certain bacterial resistance or allergic reactions in the consuming population.
In order to achieve this, the study carried out by the UGR [http://www.ugr.es], used techniques that have not been much explored in these fields. Cathodoluminiscence detection (CL) connected to Flow Injection Analysis (FIA) and High Performance Liquid Chromatography (HPCL), or Capillary Electrophoresis (CE) with UV/Vis detection using an online preconcentration technique in the capillary itself, or detection via Mass Spectometry (MS). MS can also unequivocally identify the analysed compounds. Research has been specifically based on carbamates, a widely used pesticide family, and on sulfonamides, a group of wide-spectrum antibiotics commonly used in medicine and veterinary science.
Researchers point out that methods developed in this work could be applied in the future to routine analysis for this kind of residue control in plant foods and foods of animal origin, in Quality and Alimentary Safety laboratories, or in the detection of such contaminants in waters of varied sources. “These methods definitely constitute interesting alternatives to the already established and less sensitive methods which imply a greater consumption of organic solvents and generate more contaminant residues,” the author of the thesis points out.
FQM-302 research group has been working on the proposal of methods of detecting contaminant residues in foods and in the environment for several years. Currently work is being carried out in different doctoral theses which looks at the study of other pesticide families and their degradation products, as well as the study of other antibiotics such as quinolones and beta-lactams using the methods mentioned above.
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23.03.2018 | Cold Spring Harbor Laboratory
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Satellites in near-Earth orbit are at risk due to the steady increase in space debris. But their mission in the areas of telecommunications, navigation or weather forecasts is essential for society. Fraunhofer FHR therefore develops radar-based systems which allow the detection, tracking and cataloging of even the smallest particles of debris. Satellite operators who have access to our data are in a better position to plan evasive maneuvers and prevent destructive collisions. From April, 25-29 2018, Fraunhofer FHR and its partners will exhibit the complementary radar systems TIRA and GESTRA as well as the latest radar techniques for space observation across three stands at the ILA Berlin.
The "traffic situation" in space is very tense: the Earth is currently being orbited not only by countless satellites but also by a large volume of space...
An international team of researchers has discovered a new anti-cancer protein. The protein, called LHPP, prevents the uncontrolled proliferation of cancer cells in the liver. The researchers led by Prof. Michael N. Hall from the Biozentrum, University of Basel, report in “Nature” that LHPP can also serve as a biomarker for the diagnosis and prognosis of liver cancer.
The incidence of liver cancer, also known as hepatocellular carcinoma, is steadily increasing. In the last twenty years, the number of cases has almost doubled...
In just a few weeks from now, the Chinese space station Tiangong-1 will re-enter the Earth's atmosphere where it will to a large extent burn up. It is possible that some debris will reach the Earth's surface. Tiangong-1 is orbiting the Earth uncontrolled at a speed of approx. 29,000 km/h.Currently the prognosis relating to the time of impact currently lies within a window of several days. The scientists at Fraunhofer FHR have already been monitoring Tiangong-1 for a number of weeks with their TIRA system, one of the most powerful space observation radars in the world, with a view to supporting the German Space Situational Awareness Center and the ESA with their re-entry forecasts.
Following the loss of radio contact with Tiangong-1 in 2016 and due to the low orbital height, it is now inevitable that the Chinese space station will...
Fraunhofer Institute for Organic Electronics, Electron Beam and Plasma Technology FEP, provider of research and development services for OLED lighting solutions, announces the founding of the “OLED Licht Forum” and presents latest OLED design and lighting solutions during light+building, from March 18th – 23rd, 2018 in Frankfurt a.M./Germany, at booth no. F91 in Hall 4.0.
They are united in their passion for OLED (organic light emitting diodes) lighting with all of its unique facets and application possibilities. Thus experts in...
A new scenario seeking to explain how Mars' putative oceans came and went over the last 4 billion years implies that the oceans formed several hundred million...
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