Forum for Science, Industry and Business

Sponsored by:     3M 
Search our Site:

 

A New X-Ray Microscope for Nanoscale Imaging

02.03.2015

Delivering the capability to image nanostructures and chemical reactions down to nanometer resolution requires a new class of x-ray microscope that can perform precision microscopy experiments using ultra-bright x-rays from the National Synchrotron Light Source II (NSLS-II) at Brookhaven National Laboratory.

This groundbreaking instrument, designed to deliver a suite of unprecedented x-ray imaging capabilities for the Hard X-ray Nanoprobe (HXN) beamline, brings researchers one step closer to the ultimate goal of nanometer resolution at NSLS-II, a U.S. Department of Energy Office of Science User Facility.


Brookhaven National Laboratory

Multi-layer Laue lens module inside the vacuum chamber of the microscope installed at the Hard X-ray Nanoprobe beamline at NSLS-II.

The microscope manipulates novel nanofocusing optics called multilayer Laue lenses (MLL) — incredibly precise lenses grown one atomic layer at a time — which produce a tiny x-ray beam that is currently about 10 nanometers in size. Focusing an x-ray beam to that level means being able to see the structures on that length scale, whether they are proteins in a biological sample, or the inner workings of a fuel cell catalyst.

The team of scientists who built this microscope aren’t stopping there; they are working toward making the focused x-ray beam spot even smaller in the future. The microscope they developed produces x-ray images by scanning a sample while collecting various x-ray signals emerging from the sample.

Analysis of these signals helps researchers understand crucial information about the materials they are examining: density, elemental composition, chemical state, and the crystalline structure of the sample.

Getting a clear image at this scale requires extremely high stability of the microscope to minimize vibrations and to reduce possible thermal drifts, changes in the microscope due to heat. It requires over twenty piezo motors — very fine motors that produce motion when electric currents are fed into piezo crystals — controlled down to nanometer-scale precision, crammed into a tight space about the size of a coffee maker, to meet its functionalities.

“This instrument incorporates most recent developments in interferometric sensing, nanoscale motion, and position control. Recorded drifts of two nanometers per hour are unprecedented and set a new benchmark for x-ray microscopy systems,” said Evgeny Nazaretski, a physicist at NSLS-II who spearheaded the development of the microscope.

After construction, the MLL module, a key component of the HXN x-ray microscope, was tested at the Diamond Light Source Beamline I-13L for extensive x-ray performance measurements. These measurements confirmed the stability and reliability of the new MLL system. Results are being published in the March issue of the Journal of Synchrotron Radiation.

Hanfei Yan, a co-author of the paper, added, “We are grateful to our collaborators from Argonne National Laboratory who shared their technical expertise from the beginning of this project and also to collaborators from the Diamond Light Source who wholeheartedly supported the x-ray experiments.”

“This instrument is a critical link connecting NSLS-II’s bright x-rays to unprecedented nanoscale x-ray imaging capabilities, which we believe will lead to many groundbreaking scientific discoveries”, stressed Yong Chu, the Group Leader of the Hard X-ray Nanoprobe Beamline at NSLS-II. The HXN beamline and the HXN x-ray microscope are currently being commissioned and will be available for user experiments later this year.

This work is published in the Journal of Synchrotron Radiation.

Brookhaven National Laboratory is supported by the Office of Science of the U.S. Department of Energy. The Office of Science is the single largest supporter of basic research in the physical sciences in the United States, and is working to address some of the most pressing challenges of our time. For more information, please visit science.energy.gov.

Contact Information
Chelsea Whyte
Public Affairs Representative
cwhyte@bnl.gov
Phone: 6313448671

Chelsea Whyte | newswise
Further information:
http://www.bnl.gov

Further reports about: Brookhaven Diamond Energy MLL Microscope Science Synchrotron beamline experiments measurements nanoscale sample

More articles from Physics and Astronomy:

nachricht From rocks in Colorado, evidence of a 'chaotic solar system'
23.02.2017 | University of Wisconsin-Madison

nachricht Prediction: More gas-giants will be found orbiting Sun-like stars
22.02.2017 | Carnegie Institution for Science

All articles from Physics and Astronomy >>>

The most recent press releases about innovation >>>

Die letzten 5 Focus-News des innovations-reports im Überblick:

Im Focus: Breakthrough with a chain of gold atoms

In the field of nanoscience, an international team of physicists with participants from Konstanz has achieved a breakthrough in understanding heat transport

In the field of nanoscience, an international team of physicists with participants from Konstanz has achieved a breakthrough in understanding heat transport

Im Focus: DNA repair: a new letter in the cell alphabet

Results reveal how discoveries may be hidden in scientific “blind spots”

Cells need to repair damaged DNA in our genes to prevent the development of cancer and other diseases. Our cells therefore activate and send “repair-proteins”...

Im Focus: Dresdner scientists print tomorrow’s world

The Fraunhofer IWS Dresden and Technische Universität Dresden inaugurated their jointly operated Center for Additive Manufacturing Dresden (AMCD) with a festive ceremony on February 7, 2017. Scientists from various disciplines perform research on materials, additive manufacturing processes and innovative technologies, which build up components in a layer by layer process. This technology opens up new horizons for component design and combinations of functions. For example during fabrication, electrical conductors and sensors are already able to be additively manufactured into components. They provide information about stress conditions of a product during operation.

The 3D-printing technology, or additive manufacturing as it is often called, has long made the step out of scientific research laboratories into industrial...

Im Focus: Mimicking nature's cellular architectures via 3-D printing

Research offers new level of control over the structure of 3-D printed materials

Nature does amazing things with limited design materials. Grass, for example, can support its own weight, resist strong wind loads, and recover after being...

Im Focus: Three Magnetic States for Each Hole

Nanometer-scale magnetic perforated grids could create new possibilities for computing. Together with international colleagues, scientists from the Helmholtz Zentrum Dresden-Rossendorf (HZDR) have shown how a cobalt grid can be reliably programmed at room temperature. In addition they discovered that for every hole ("antidot") three magnetic states can be configured. The results have been published in the journal "Scientific Reports".

Physicist Dr. Rantej Bali from the HZDR, together with scientists from Singapore and Australia, designed a special grid structure in a thin layer of cobalt in...

All Focus news of the innovation-report >>>

Anzeige

Anzeige

Event News

Booth and panel discussion – The Lindau Nobel Laureate Meetings at the AAAS 2017 Annual Meeting

13.02.2017 | Event News

Complex Loading versus Hidden Reserves

10.02.2017 | Event News

International Conference on Crystal Growth in Freiburg

09.02.2017 | Event News

 
Latest News

Stingless bees have their nests protected by soldiers

24.02.2017 | Life Sciences

New risk factors for anxiety disorders

24.02.2017 | Life Sciences

MWC 2017: 5G Capital Berlin

24.02.2017 | Trade Fair News

VideoLinks
B2B-VideoLinks
More VideoLinks >>>