Forum for Science, Industry and Business

Sponsored by:     3M 
Search our Site:

 

NIST develops rapid method for judging nanotube purity

06.02.2007
Researchers at the National Institute of Standards and Technology (NIST) have developed a sensitive new method for rapidly assessing the quality of carbon nanotubes.

Initial feasibility tests show that the method not only is faster than the standard analytic technique but also effectively screens much smaller samples for purity and consistency and better detects sample variability.

Carbon nanotubes have unique properties, and thermal and electrical conductance, that could be useful in fields such as aerospace, microelectronics and biotechnology. However, these properties may vary widely depending on nanotube dimensions, uniformity and chemical purity. Nanotube samples typically contain a significant percentage of more ordinary forms of carbon as well as metal particles left over from catalysts used in manufacturing. The new NIST method, described at a conference last week,* involves spraying nanotube coatings onto a quartz crystal, gradually heating the coated crystal, and measuring the change in its resonant frequency as different forms of carbon vaporize. The frequency changes in proportion to the mass of the coating, and scientists use this as a measure of stability at different temperatures to gauge consistency among samples. The quartz crystal technique, which can reveal mass changes of just a few nanograms, already is used in other contexts to detect toxic gases and measure molecular interactions.

NIST researchers tested dozens of samples from a batch of commercial single-walled carbon nanotubes, comparing results of the new method with those from a standard technique, thermogravimetric analysis, and confirming results with scanning electron microscopy. Both methods revealed that the samples contained large amounts of amorphous carbon as well as residual metal particles. But the quartz crystal method could obtain results from just micrograms of material, compared to milligrams for thermogravimetric analysis, and also revealed several orders of magnitude more variability in the samples tested. The new technique also uses simpler equipment.

Although the differences among nanotube samples may appear subtle, they may still affect product viability, because even small variations in material composition can affect electrical and thermal behavior, and lack of uniformity may demand higher loads of nanotubes, which are expensive. NIST scientists carried out the tests with the help of students from the University of Colorado-Boulder and Rensselaer Polytechnic Institute, Troy, N.Y.

Laura Ost | EurekAlert!
Further information:
http://www.nist.gov

More articles from Process Engineering:

nachricht New technology for ultra-smooth polymer films
28.06.2018 | Fraunhofer-Institut für Organische Elektronik, Elektronenstrahl- und Plasmatechnik FEP

nachricht Diamond watch components
18.06.2018 | Schweizerischer Nationalfonds SNF

All articles from Process Engineering >>>

The most recent press releases about innovation >>>

Die letzten 5 Focus-News des innovations-reports im Überblick:

Im Focus: Future electronic components to be printed like newspapers

A new manufacturing technique uses a process similar to newspaper printing to form smoother and more flexible metals for making ultrafast electronic devices.

The low-cost process, developed by Purdue University researchers, combines tools already used in industry for manufacturing metals on a large scale, but uses...

Im Focus: First evidence on the source of extragalactic particles

For the first time ever, scientists have determined the cosmic origin of highest-energy neutrinos. A research group led by IceCube scientist Elisa Resconi, spokesperson of the Collaborative Research Center SFB1258 at the Technical University of Munich (TUM), provides an important piece of evidence that the particles detected by the IceCube neutrino telescope at the South Pole originate from a galaxy four billion light-years away from Earth.

To rule out other origins with certainty, the team led by neutrino physicist Elisa Resconi from the Technical University of Munich and multi-wavelength...

Im Focus: Magnetic vortices: Two independent magnetic skyrmion phases discovered in a single material

For the first time a team of researchers have discovered two different phases of magnetic skyrmions in a single material. Physicists of the Technical Universities of Munich and Dresden and the University of Cologne can now better study and understand the properties of these magnetic structures, which are important for both basic research and applications.

Whirlpools are an everyday experience in a bath tub: When the water is drained a circular vortex is formed. Typically, such whirls are rather stable. Similar...

Im Focus: Breaking the bond: To take part or not?

Physicists working with Roland Wester at the University of Innsbruck have investigated if and how chemical reactions can be influenced by targeted vibrational excitation of the reactants. They were able to demonstrate that excitation with a laser beam does not affect the efficiency of a chemical exchange reaction and that the excited molecular group acts only as a spectator in the reaction.

A frequently used reaction in organic chemistry is nucleophilic substitution. It plays, for example, an important role in in the synthesis of new chemical...

Im Focus: New 2D Spectroscopy Methods

Optical spectroscopy allows investigating the energy structure and dynamic properties of complex quantum systems. Researchers from the University of Würzburg present two new approaches of coherent two-dimensional spectroscopy.

"Put an excitation into the system and observe how it evolves." According to physicist Professor Tobias Brixner, this is the credo of optical spectroscopy....

All Focus news of the innovation-report >>>

Anzeige

Anzeige

VideoLinks
Industry & Economy
Event News

Leading experts in Diabetes, Metabolism and Biomedical Engineering discuss Precision Medicine

13.07.2018 | Event News

Conference on Laser Polishing – LaP: Fine Tuning for Surfaces

12.07.2018 | Event News

11th European Wood-based Panel Symposium 2018: Meeting point for the wood-based materials industry

03.07.2018 | Event News

 
Latest News

A smart safe rechargeable zinc ion battery based on sol-gel transition electrolytes

20.07.2018 | Power and Electrical Engineering

Reversing cause and effect is no trouble for quantum computers

20.07.2018 | Information Technology

Princeton-UPenn research team finds physics treasure hidden in a wallpaper pattern

20.07.2018 | Materials Sciences

VideoLinks
Science & Research
Overview of more VideoLinks >>>