Forum for Science, Industry and Business

Sponsored by:     3M 
Search our Site:

 

World’s smallest universal material testing system

23.09.2005


The design, development and manufacturing of revolutionary products such as the automobile, airplane and computer owe a great deal of their success to the large-scale material testing systems (MTS) that have provided engineers and designers with a fundamental understanding of the mechanical behavior of various materials and structures.



In the world of nanotechnology, however, where the mechanical characterization of materials and structures takes place on the scale of atoms and molecules, the existing material testing systems are useless. The development of a universal nanoscale material testing system (n-MTS), which could fit in existing electron microscopes (instruments that can magnify images approximately one million times) and possess the resolution and accuracy needed to mechanically test nanoscale objects, has been a major challenge within the scientific community.

Now researchers at Northwestern University have designed and built the first complete micromachine that makes possible the investigation of nanomechanics phenomena in real time. The findings are published online this week by the Proceedings of the National Academy of Sciences (PNAS). The machine, which can fit in tiny spaces as required by in situ transmission electron microscopy (TEM), successfully characterized the mechanical properties of nanowires and carbon nanotubes.


The n-MTS developed by Horacio D. Espinosa, professor of mechanical engineering, and his colleagues consists of an actuator and a load sensor fabricated by means of micro technology (a derivative of the computer industry). The load sensor is based on differential capacitive sensing, which provides a load resolution of about 10 nano Newtons. This is the first nanoscale material testing system that provides continuous observation of specimen deformation and failure with sub-nanometer resolution while simultaneously measuring electronically the applied forces with nano-Newton resolution. The integration of electro-mechanical and thermo-mechanical components at the micro scale made the achievement possible.

One of the challenges overcome by the University researchers was the integration of micro-electro-mechanical systems (MEMS) and circuits for measurement of electronic signals. They solved this problem by using a double-chip architecture consisting of a MEMS chip and a microelectronic sensing chip.

Another challenge overcome by the team was the mounting of individual nanostructures on the testing device. Using a nanomanipulator inside a dual-beam scanning electron microscope and focused ion beam apparatus (a new tool available to nanoscientists) the researchers picked up nanostructures, cut them to the desired length and nanowelded the structures onto the n-MTS using electron-beam-induced deposition of platinum.

As reported in the PNAS paper, the system capabilities were demonstrated by in situ electron microscopy testing of free-standing polysilicon films, metallic nanowires and carbon nanotubes (CNTs). Espinosa’s team achieved the first real-time instrumented in situ transmission electron microscopy observation of CNTs failure under tensile loading.

In 1959, Nobel Laureate Richard Feynman delivered a talk at the California Institute of Technology entitled "There is Plenty of Room at the Bottom" in which he envisioned the possibility of making very small machines. "Our MEMS-based nanoscale material testing system represents another milestone along the path of miniaturization anticipated by Feynman," said Espinosa. "We expect it will have a similar impact and produce the same level of opportunities as the development of the universal testing machine had in the last century."

The n-MTS can be potentially applied to characterize the mechanical, thermal and electro-mechanical properties not only of nanowires and nanotubes but also of a large number of organic materials, including DNA, proteins and nanofibers.

Megan Fellman | EurekAlert!
Further information:
http://www.northwestern.edu

More articles from Materials Sciences:

nachricht New biomaterial could replace plastic laminates, greatly reduce pollution
21.09.2017 | Penn State

nachricht Stopping problem ice -- by cracking it
21.09.2017 | Norwegian University of Science and Technology

All articles from Materials Sciences >>>

The most recent press releases about innovation >>>

Die letzten 5 Focus-News des innovations-reports im Überblick:

Im Focus: The pyrenoid is a carbon-fixing liquid droplet

Plants and algae use the enzyme Rubisco to fix carbon dioxide, removing it from the atmosphere and converting it into biomass. Algae have figured out a way to increase the efficiency of carbon fixation. They gather most of their Rubisco into a ball-shaped microcompartment called the pyrenoid, which they flood with a high local concentration of carbon dioxide. A team of scientists at Princeton University, the Carnegie Institution for Science, Stanford University and the Max Plank Institute of Biochemistry have unravelled the mysteries of how the pyrenoid is assembled. These insights can help to engineer crops that remove more carbon dioxide from the atmosphere while producing more food.

A warming planet

Im Focus: Highly precise wiring in the Cerebral Cortex

Our brains house extremely complex neuronal circuits, whose detailed structures are still largely unknown. This is especially true for the so-called cerebral cortex of mammals, where among other things vision, thoughts or spatial orientation are being computed. Here the rules by which nerve cells are connected to each other are only partly understood. A team of scientists around Moritz Helmstaedter at the Frankfiurt Max Planck Institute for Brain Research and Helene Schmidt (Humboldt University in Berlin) have now discovered a surprisingly precise nerve cell connectivity pattern in the part of the cerebral cortex that is responsible for orienting the individual animal or human in space.

The researchers report online in Nature (Schmidt et al., 2017. Axonal synapse sorting in medial entorhinal cortex, DOI: 10.1038/nature24005) that synapses in...

Im Focus: Tiny lasers from a gallery of whispers

New technique promises tunable laser devices

Whispering gallery mode (WGM) resonators are used to make tiny micro-lasers, sensors, switches, routers and other devices. These tiny structures rely on a...

Im Focus: Ultrafast snapshots of relaxing electrons in solids

Using ultrafast flashes of laser and x-ray radiation, scientists at the Max Planck Institute of Quantum Optics (Garching, Germany) took snapshots of the briefest electron motion inside a solid material to date. The electron motion lasted only 750 billionths of the billionth of a second before it fainted, setting a new record of human capability to capture ultrafast processes inside solids!

When x-rays shine onto solid materials or large molecules, an electron is pushed away from its original place near the nucleus of the atom, leaving a hole...

Im Focus: Quantum Sensors Decipher Magnetic Ordering in a New Semiconducting Material

For the first time, physicists have successfully imaged spiral magnetic ordering in a multiferroic material. These materials are considered highly promising candidates for future data storage media. The researchers were able to prove their findings using unique quantum sensors that were developed at Basel University and that can analyze electromagnetic fields on the nanometer scale. The results – obtained by scientists from the University of Basel’s Department of Physics, the Swiss Nanoscience Institute, the University of Montpellier and several laboratories from University Paris-Saclay – were recently published in the journal Nature.

Multiferroics are materials that simultaneously react to electric and magnetic fields. These two properties are rarely found together, and their combined...

All Focus news of the innovation-report >>>

Anzeige

Anzeige

Event News

“Lasers in Composites Symposium” in Aachen – from Science to Application

19.09.2017 | Event News

I-ESA 2018 – Call for Papers

12.09.2017 | Event News

EMBO at Basel Life, a new conference on current and emerging life science research

06.09.2017 | Event News

 
Latest News

Rainbow colors reveal cell history: Uncovering β-cell heterogeneity

22.09.2017 | Life Sciences

Penn first in world to treat patient with new radiation technology

22.09.2017 | Medical Engineering

Calculating quietness

22.09.2017 | Physics and Astronomy

VideoLinks
B2B-VideoLinks
More VideoLinks >>>